A displacement sensing nanoindentation study of tribo-mechanical properties of the Ni–Co system

An analysis of the tribo-mechanical properties of the Ni–Co system, at the submicrometric contact scale, is conducted using displacement sensing nanoindentation. In particular, the influence of contact depth and surface finishing methods on the hardness, H, and Youngʹs modulus, E, of the materials is analysed. Mechanically and electrolitically polished samples were tested with a conospherical indenter using a range of loads between 0.05 and 10 mN. It is shown that the hardness of these materials depends on the surface finishing method and increases with decreasing contact depth, while the Youngʹs modulus is relatively insensitive to contact depth. Furthermore, sample polycrystallinity leads to a large scattering of hardness values in Co-rich samples and of Youngʹs modulus values in Ni-rich ones. The combined parametric ratio H/E, which can be related to the tribological behaviour of the material, was found to be higher in samples with Co content larger than 80 wt.%.