Author/Authors :
Arabi، F. نويسنده Department of chemistry, Saveh Branch, Islamic Azad University, Saveh, Iran , , Emami Meibodi، A. نويسنده Department of chemistry, Karaj Branch, Islamic Azad University, Karaj, Iran , , Aflaki، F. نويسنده Nuclear Science Research School, Nuclear Science and Technology Research Institute, Tehran, Iran ,
Abstract :
In this work preconcentration of the Zn ions was investigated in water sample by Dispersive liquid- liquid micro extraction (DLLME) using chloroform as an extraction solvent, methanol as a disperser solvent and 8-Hydroxyquinoline as a chelating agent. The determination of extracted ions was done by graphite furnace atomic absorption spectrometry. The influence of various analytical parameters including pH, extraction and disperser solvent type and volume and concentration of the chelating agent on the extraction efficiency of analyses was investigated. After extraction, the enrichment factor was 26 and the detection limit of the method was 0.0033 ?g l-1 and the relative standard deviations (R.S.D) for five determinations of 1 ng/ml Zn were 7.41%.
