Title of article
Single crystal X-ray structure of 3-amino-5-(4-chlorophenyl)pyridazine-4-carbonitrile
Author/Authors
Khalafy، Jabbar نويسنده Department of Organic Chemistry, Faculty of Chemistry, Urmia University, Urmia 57154, Iran , , Farajzadeh، Somaye نويسنده Department of Organic Chemistry, Faculty of Chemistry, Urmia University, Urmia 57154, Iran , , Poursattar Marjani، Ahmad نويسنده , , Yaghoobnejad Asl، Hooman نويسنده Department of Chemistry, Missouri University of Science and Technology, Rolla, MO 65409, USA ,
Issue Information
فصلنامه با شماره پیاپی 9 سال 2014
Pages
6
From page
1
To page
6
Abstract
The title compound 3-amino-5-(4-chlorophenyl)pyridazine-4-carbonitrile was prepared by a one-pot three-component reaction of malononitrile with corresponding arylglyoxal in the presence of hydrazine hydrate at room temperature in water and ethanol. Its structure was also con?rmed by its IR, 1H, 13C-NMR, Mass spectral data and elemental analysis. The compound was crystallized in the monoclinic system, space group P21/c, a = 3.817(3) ?, b = 13.533(10) ?, c = 19.607(15) ?, B = 93.401(10)°, Z=4, R1 = 0.0906 and wR2 = 0.1422. The crystal structure of the compound also shows a weak intermolecular interaction between N1 atom of one molecule and N3 atom of the other molecule.
Journal title
Current Chemistry Letters
Serial Year
2014
Journal title
Current Chemistry Letters
Record number
1037977
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