Title of article
Solid-phase synthesis of 15N-labeled acylpentamines as reference compounds for the MS/MS investigation of spider toxins
Author/Authors
Nikolay Manov، نويسنده , , Manuel Tzouros، نويسنده , , Laurent Bigler، نويسنده , , Stefan Bienz، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2004
Pages
5
From page
2387
To page
2391
Abstract
A solid-phase route for synthesis of 15N-labeled acylpolyamines is described. Utilizing alkylation at benzylic N-atom as a key step, 15N-atoms are incorporated by stepwise construction of the polyamine framework on the solid support. The derivatives were used as reference compounds for the investigation of the MS/MS behavior of spider toxins.
Keywords
15N-labeled , Spider toxin , Polyamine , MS/MS , Solid-phase synthesis
Journal title
Tetrahedron
Serial Year
2004
Journal title
Tetrahedron
Record number
1085061
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