Title of article :
An improved large scale synthesis of 1,4-anhydro-4-thio-d-ribitol
Author/Authors :
Noriaki Minakawa، نويسنده , , Yuka Kato، نويسنده , , Koichi Uetake، نويسنده , , Daisuke Kaga، نويسنده , , Akira Matsuda and Fuyuhiko Inagaki، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2003
Abstract :
An improved large scale synthesis of 1,4-anhydro-4-thio-d-ribitol () from d-ribose has been accomplished by combining the O-allyl and O-p-methoxybenzyl protecting groups. Compound was obtained in 31% yield in eight steps with three chromatographic separations.
Keywords :
Thiosugars , Protecting groups , Sulfides
Journal title :
Tetrahedron
Journal title :
Tetrahedron