Crystallographic and morphological relationships between β phase and the Widmanstätten and allotriomorphic α phase at special β grain boundaries in an α/β titanium alloy Original Research Article

In the present study, the relationship between the crystallographic orientations and growth directions of grain boundary-allotriomorphic-α (GB α) and secondary Widmanstätten α laths growing from the GB α at grain boundaries separating β grains with specific misorientations has been examined. These relationships have been determined using a variety of characterization techniques, including scanning electron microscopy, orientation imaging microscopy, transmission electron microscopy (TEM) and a dual-beam focused ion beam instrument to provide site-selected TEM foils. Two very interesting cases, one in which the two adjacent β grains are rotated mutually by approximately 10.5° about a common 〈1 1 0〉 direction and the other in which the two β grains are in a twin relationship, i.e. a 60° rotation about a common 〈1 1 1〉 direction, have been studied. It was discovered that the α laths growing into two adjacent β grains from the common grain boundary may have the same orientation in both grains, while they may have either large (∼88.8°) or small (28.8°) angular differences in growth directions in the two adjacent β grains, depending on the relative misorientation of the β grains. The growth directions of the α laths growing from such boundaries are explained on the basis of the Burgers orientation relationship between the Widmanstätten α and the β phases and the interfacial structure proposed previously by various workers.