Title of article
Microwave-assisted synthesis of [Os2Cl3(PEt2Ph)6]Cl, featuring the first reported X-ray crystal structure
Author/Authors
Bennett J. Tardiff، نويسنده , , Andreas Decken، نويسنده , , G. Sean McGrady، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2008
Pages
3
From page
44
To page
46
Abstract
The microwave-assisted synthesis of [Os2Cl3(PEt2Ph)6]Cl, a useful intermediate in osmium chemistry, was performed in a minimum amount of time under aerobic conditions, and the product readily crystallized from the reaction solution. Its single crystal X-ray structure and a full characterization by NMR spectroscopy are reported for the first time.
Keywords
Osmium , X-ray structure , Phosphine , Microwave synthesis
Journal title
Inorganic Chemistry Communications
Serial Year
2008
Journal title
Inorganic Chemistry Communications
Record number
1317625
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