Title of article
Synthesis and characterization of hexa-n-propylcyclotriphosphazene
Author/Authors
John R. Klaehn، نويسنده , , Eric S. Peterson، نويسنده , , Thomas A. Luther، نويسنده , , Raymond D. Larsen، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2006
Pages
4
From page
1697
To page
1700
Abstract
Dynamic vacuum thermolysis of (CH3)3SiN = P(n-Pr)2(OPh) yielded hexa-n-propylcyclotriphosphazene, [N = P(n-Pr)2]3. It was found that pure [N = P(n-Pr)2]3is insoluble in most solvents, however, [N = P(n-Pr)2]3 can be crystallized directly from the crude reaction mixture using hot hexanes. The molecular structure of hexa-n-propylcyclotriphosphazene has been determined by single-crystal X-ray diffraction and multinuclear NMR studies.
Keywords
Phosphazene , Single-crystal , X-ray structure , Characterization , Synthesis
Journal title
INORGANICA CHIMICA ACTA
Serial Year
2006
Journal title
INORGANICA CHIMICA ACTA
Record number
1323527
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