Title of article
Improvement of X-ray powder diffraction patterns of the spin transition polymer [Fe(Htrz)3](ClO4)2.1.85H2O
Author/Authors
Smit، E. نويسنده , , Manoun، B. نويسنده , , Verryn، S. M. C. نويسنده , , Waal، D. de نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2001
Pages
-36
From page
37
To page
0
Abstract
Using a recent proposed analysis procedure for quantitative phase determination by X-ray powder diffraction, YBa2Cu3O7-x solid state formation reaction kinetics at 900 °C was studied. Although there was the presence of partial amorphous components, it was possible to determine a reaction route for the synthesis of the title compound from X-ray powder diffraction data collected at various stages of the thermal treatment and using the Rietveld method for the quantitative determination of the phase composition.
Keywords
powder diffraction , Decomposition , lithium copper oxide , crystal growth , LiCu3O3 , LiCu2O2 , Phase diagram , density
Journal title
POWDER DIFFRACTION
Serial Year
2001
Journal title
POWDER DIFFRACTION
Record number
15208
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