Title of article
Effect of solvents on the fumonisins analysis by high-performance liquid chromatography with AccQ.Fluor as the derivatizing reagent
Author/Authors
Velلzquez، نويسنده , , Carlos and Llovera، نويسنده , , Monserrat and Plana، نويسنده , , Jordi and Canela، نويسنده , , Ramon، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2000
Pages
4
From page
469
To page
472
Abstract
The effect of several solvent systems on the chromatographic response of fumonisin B1 and B2 derived with 6-aminoquinolyl-N-hydroxysuccinimidyl carbamate (AccQ.Fluor) is described. Naturally contaminated corn samples were extracted and purified by a standard method. Then, samples were dissolved in different solvents, derived with AccQ.Fluor reagent and analysed using HPLC. Results were solvent dependent, methanol being the best one among all assayed solvents for both fumonisins studied and acetonitrile the poorest. o-Phthaldialdehyde (OPA) reagent was used as a reference method.
Keywords
o-Phthaldialdehyde , AccQ.Fluor reagent , fumonisin
Journal title
Journal of Chromatography A
Serial Year
2000
Journal title
Journal of Chromatography A
Record number
1526893
Link To Document