Title of article
Synthesis and 19F NMR study of RF-oleic acid-F13
Author/Authors
Buchanan، نويسنده , , Gerald W. and Smits، نويسنده , , Rufus and Munteanu، نويسنده , , Elena، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2003
Pages
5
From page
255
To page
259
Abstract
A seven-step synthesis of Z-13,13,14,14,15,15,16,16,17,17,18,18,18-tridecafluoro-octadec-9-enoic acid (oleic acid-F13) is reported. The key step is a Wittig reaction to form the C9–C10 double bond with a Z:E isomeric ratio greater than 20:1. The 19F nuclear magnetic resonance (NMR) spectrum is included and unambiguous assignments have been made with the aid of 19F–19F correlation NMR spectroscopy (COSY spectra).
Keywords
Terminally perfluorinated oleic acid , 19F NMR
Journal title
Journal of Fluorine Chemistry
Serial Year
2003
Journal title
Journal of Fluorine Chemistry
Record number
1607791
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