Title of article :
Preparative-scale synthesis of 3,3,3-trifluoropropene oxide
Author/Authors :
Ramachandran، نويسنده , , P. Veeraraghavan and Padiya، نويسنده , , Kamlesh J. Padiya، نويسنده ,
Issue Information :
روزنامه با شماره پیاپی سال 2007
Abstract :
Bromination of 3,3,3-trifluoropropene in 20% oleum, followed by treatment with acetic acid furnishes 2-bromo-3,3,3-trifluoropropyl acetate in quantitative yield, which upon acid hydrolysis and cyclization with alkali affords 3,3,3-trifluoropropene oxide (TFPO) in 63% overall yield.
Keywords :
3 , 3 , 3-trifluoropropene , 3 , 3 , 3-Trifluoropropene oxide , Oxirane , Silver acetate , Bromination , Bromoacetoxylation
Journal title :
Journal of Fluorine Chemistry
Journal title :
Journal of Fluorine Chemistry
