Title of article
Analysis of 2-deuterated isopentenyl alcohols by 1H NMR of chiral esters
Author/Authors
Giner، نويسنده , , José-Luis and Kiemle، نويسنده , , David and Zuniga، نويسنده , , Daniel J، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2002
Pages
3
From page
1175
To page
1177
Abstract
A convenient procedure is presented whereby the chirality of isopentenyl alcohols labeled with deuterium in the 2-position can be determined by 1H NMR analysis of their chiral esters. The MTPA, MPA and O-acetylmandelate esters were investigated in a series of NMR solvents. The best results were obtained using the O-acetylmandelates in C6D6 with homodecoupling of the 1-position.
Journal title
Tetrahedron Letters
Serial Year
2002
Journal title
Tetrahedron Letters
Record number
1649855
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