Synthesis of fluorous azodicarboxylates: towards cleaner Mitsunobu reactions
Author/Authors :
Dobbs، نويسنده , , Adrian P and McGregor-Johnson، نويسنده , , Caroline، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2002
Pages :
4
From page :
2807
To page :
2810
Abstract :
The synthesis of a fluorous analogue of diethyl azodicarboxylate (DEAD) is described and preliminary results for its use in the Mitsunobu reaction given. Use of fluorous extraction methods have shown that chromatography is not necessary for reaction purification.
