Title of article
Synthesis of mucin-type glycopeptide (β hCG 130–145) by on-resin fragment condensation of the glycopeptide segments carrying unmasked oligosaccharides
Author/Authors
Ichiyanagi، نويسنده , , Tsuyoshi and Takatani، نويسنده , , Maki and Sakamoto، نويسنده , , Kimitoshi and Nakahara، نويسنده , , Yuko and Ito، نويسنده , , Yukishige and Hojo، نويسنده , , Hironobu and Nakahara، نويسنده , , Yoshiaki، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2002
Pages
4
From page
3297
To page
3300
Abstract
Use of amino acid pentafluorophenyl esters was found effective for chemoselective N-acylation in the peptide elongation. On-resin fragment condensation between 9 and 13 using DCC-PfpOH as an activator afforded coupling product 1 in good yield.
Keywords
Condensations , Pentafluorophenyl esters , Glycopeptides
Journal title
Tetrahedron Letters
Serial Year
2002
Journal title
Tetrahedron Letters
Record number
1651407
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