Title of article :
Expedient microwave deuteration of estrone in CF3COOD
Author/Authors :
Kiuru، نويسنده , , Paula S and Wنhنlن، نويسنده , , Kristiina، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2002
Abstract :
A rapid and efficient deuteration procedure was developed for estrone. Irradiation of estrone in CF3COOD in a microwave oven gave [2,4,16,16-2H4]-estrone in 95% yield. Ultrasound and CF3COOD reflux deuterations of estrone were also studied.
Journal title :
Tetrahedron Letters
Journal title :
Tetrahedron Letters