• Title of article

    Chemoselective peptide bond formation using formyl-substituted nitrophenylthio ester

  • Author/Authors

    Ishiwata، نويسنده , , Akihiro and Ichiyanagi، نويسنده , , Tsuyoshi and Takatani، نويسنده , , Maki and Ito، نويسنده , , Yukishige، نويسنده ,

  • Issue Information
    هفته نامه با شماره پیاپی سال 2003
  • Pages
    4
  • From page
    3187
  • To page
    3190
  • Abstract
    A novel method for peptide bond formation utilizing amino acid 2-formyl-4-nitrophenylthio ester has been developed. The reaction can be performed in water-containing media and is compatible with various types of amino acid side-chain functional groups. Use of N-methylmaleinimide as an additive is essential for the reaction to proceed with high efficiency. It captures liberated formyl-substituted thiophenol through 1,4-addition followed by aldol cyclization.
  • Journal title
    Tetrahedron Letters
  • Serial Year
    2003
  • Journal title
    Tetrahedron Letters
  • Record number

    1661706