Author/Authors :
Spilstead، نويسنده , , Kara B. and Learey، نويسنده , , Jessica J. and Doeven، نويسنده , , Egan H. and Barbante، نويسنده , , Gregory J. and Mohr، نويسنده , , Stephan and Barnett، نويسنده , , Neil W. and Terry، نويسنده , , Jessica M. and Hall، نويسنده , , Robynne M. and Francis، نويسنده , , Paul S.، نويسنده ,
Abstract :
Herein we explore modern fabrication techniques for the development of chemiluminescence detection flow-cells with features not attainable using the traditional coiled tubing approach. This includes the first 3D-printed chemiluminescence flow-cells, and a milled flow-cell designed to split the analyte stream into two separate detection zones within the same polymer chip. The flow-cells are compared to conventional detection systems using flow injection analysis (FIA) and high performance liquid chromatography (HPLC), with the fast chemiluminescence reactions of an acidic potassium permanganate reagent with morphine and a series of adrenergic phenolic amines.
Keywords :
Flow-cells , Chemiluminescence , 3D-printing , Acidic potassium permanganate , Flow injection analysis , CNC milling
