Title of article
Thermoluminescence of combustion synthesized yttrium oxide
Author/Authors
Lakshminarasappa، نويسنده , , B.N. and Jayaramaiah، نويسنده , , J.R. and Nagabhushana، نويسنده , , B.M.، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2012
Pages
4
From page
7
To page
10
Abstract
Pure yttrium oxide (Y2O3) was prepared by solution combustion technique using disodium ethylene diamine tetra acetic acid (EDTA-Na2) as fuel at ~ 350 °C. Powder X-ray diffraction (PXRD) pattern of Y2O3 revealed cubic crystalline structure with crystallite size in the range of 18–23 nm. The scanning electron microscopy (SEM) indicated the foamy and fluffy nature of the sample. Fourier transformed infrared spectroscopy (FTIR) revealed four prominent absorption with peaks at 3395, 1433, 875 and 566 cm− 1. From the optical absorption studies the energy gap of the synthesized sample was found to be 5.72 eV. Two well resolved thermoluminescence (TL) glows with peaks at 475 and 626 K were observed in γ-irradiated Y2O3. The glow curves were analyzed and the average activation energy was found to be 0.505 and 0.977 eV respectively.
Keywords
Nanoparticles , Scanning electron microscopy , Combustion synthesis , THERMOLUMINESCENCE , oxides
Journal title
Powder Technology
Serial Year
2012
Journal title
Powder Technology
Record number
1700990
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