Title of article
Synthesis and characterization of LiFePO4 prepared by sol–gel technique
Author/Authors
Sanchez، نويسنده , , M.A.E. and Brito، نويسنده , , G.E.S. and Fantini، نويسنده , , M.C.A. and Goya، نويسنده , , G.F. and Matos، نويسنده , , J.R.، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2006
Pages
4
From page
497
To page
500
Abstract
LiFePO4 powder was synthesized by means of a new route, using a two step process. In the first step, an intermediate compound was synthesized by the sol–gel method. This precursor compound to LiFePO4 was characterized by thermal analysis (TG/DTG and DSC), Mössbauer spectroscopy, Transmission Electronic Microscopy (TEM) and Small Angle Scattering (SAXS). In the second step, the precursor was sintered and analyzed by X-ray diffraction (XRD), showing the formation of the proposed single phase material.
Keywords
DSC , LiFePO4 , Sol–gel , X-ray diffraction , M?ssbauer spectrometry , TEM , TG
Journal title
Solid State Ionics
Serial Year
2006
Journal title
Solid State Ionics
Record number
1718667
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