Author/Authors :
Berger، نويسنده , , R. and Lang، نويسنده , , H.P. and Gerber، نويسنده , , Ch and Gimzewski، نويسنده , , J.K. and Fabian، نويسنده , , J.H. and Scandella، نويسنده , , L. and Meyer، نويسنده , , E. and Güntherodt، نويسنده , , H.-J.، نويسنده ,
Abstract :
We demonstrate a new method for thermal analysis of nanogram quantities of material using a micromechanical thermogravimetric technique. The cantilever-type device uses an integrated piezoresistor to sense bending and simultaneously to ramp the temperature and control temperature cycles. It has a mass resolution in the picogram range. A quantitative analysis of the dehydration of copper–sulfate–pentahydrate (CuSO4·5H2O) is presented. The technique outperforms current thermogravimetric approaches by five orders of magnitude.