Author/Authors :
Heller، نويسنده , , Jonathan and Larsen، نويسنده , , Russell and Ernst، نويسنده , , Matthias and Kolbert، نويسنده , , Andrew C. and Baldwin، نويسنده , , Michael and Prusiner، نويسنده , , Stanley B. and Wemmer، نويسنده , , David E. and Pines، نويسنده , , Alexander، نويسنده ,
Abstract :
A protocol is presented for the determination of internuclear distances using rotational-resonance magnetization-exchange NMR in systems with inhomogeneously broadened lines. Non-linear least-square fitting procedures are used to obtain the distance, the inhomogeneous broadening, the zero-quantum relaxation time, and error estimates for these parameters. We apply this procedure to a biological system of unknown structure.
