Title of article
Preparation and evaluation of a polymer-supported Mukaiyama reagent
Author/Authors
Convers، نويسنده , , Emmanuelle and Tye، نويسنده , , Heather and Whittaker، نويسنده , , Mark، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2004
Pages
4
From page
3401
To page
3404
Abstract
The synthesis of a polymer-supported Mukaiyama reagent is described. This preparation was thoroughly optimized using a DoE approach to achieve optimum loading, and the procedure was successfully applied to prepare the supported reagent on a 10 g scale. This reagent proved to be effective for the formation of carbodiimides through the dehydration of thioureas and for a one-pot guanylation of primary amines.
Keywords
Guanidines , Mukaiyama reagent , Carbodiimide
Journal title
Tetrahedron Letters
Serial Year
2004
Journal title
Tetrahedron Letters
Record number
1841395
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