Author/Authors :
Yu، نويسنده , , Jurong and Truc، نويسنده , , Vu and Riebel، نويسنده , , Peter and Hierl، نويسنده , , Elizabeth and Mudryk، نويسنده , , Boguslaw، نويسنده ,
Abstract :
A general, practical and efficient one-pot synthesis of cyclic enecarbamates is described. The protocol proceeds via reduction of lactam carbamate with Super-Hydride®, followed by in situ dehydration with trifluoroacetic anhydride (TFAA) and diisopropylethylamine (DIPEA).