Title of article
A new method for determining positions of phenolic hydroxyl groups through silylation and application of H(Si)C triple-resonance NMR experiments
Author/Authors
Malo?، نويسنده , , Michal and Takahashi، نويسنده , , Shunya and Koshino، نويسنده , , Hiroyuki، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2007
Pages
5
From page
7586
To page
7590
Abstract
Two-dimensional triple-resonance H(Si)C NMR experiments have been applied at natural abundance to assign 13C NMR signals in silylated phenols. The method showing its great potential in determining positions of hydroxyl groups is widely applicable to signal assignment and structure elucidation of synthetic and natural phenolic compounds.
Keywords
29Si–13C long-range coupling , 29Si–1H long-range coupling , Double-INEPT , phenol
Journal title
Tetrahedron Letters
Serial Year
2007
Journal title
Tetrahedron Letters
Record number
1856954
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