Title of article
Solvent-free synthesis of 1-(p-toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-one from Dess–Martin periodinane and its synthetic utility for α-tosyloxylation of ketones
Author/Authors
Karade، نويسنده , , Nandkishor N. and Tiwari، نويسنده , , Girdharilal B. and Shinde، نويسنده , , Sandeep V. and Gampawar، نويسنده , , Sumeet V. and Kondre، نويسنده , , Jeevan M.، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2008
Pages
3
From page
3441
To page
3443
Abstract
The solvent-free synthesis of 1-(p-toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-one is reported from Dess–Martin periodinane and p-toluenesulfonic acid monohydrate using a grinding technique and is subsequently utilized for the α-tosyloxylation of a range of enolisable ketones.
Keywords
?-Tosyloxylation , PTSA , Solvent-free reactions , Dess–Martin periodinane , hypervalent iodine
Journal title
Tetrahedron Letters
Serial Year
2008
Journal title
Tetrahedron Letters
Record number
1859315
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