• Title of article

    Iron-catalyzed hydroxylation of β-ketoesters with hydrogen peroxide as oxidant

  • Author/Authors

    Li، نويسنده , , Dongmei and Schrِder، نويسنده , , Kristin and Bitterlich، نويسنده , , Bianca and Tse، نويسنده , , Man Kin and Beller، نويسنده , , Matthias، نويسنده ,

  • Issue Information
    هفته نامه با شماره پیاپی سال 2008
  • Pages
    4
  • From page
    5976
  • To page
    5979
  • Abstract
    The hydroxylation of β-ketoesters was studied using simple iron catalysts and 30 wt % hydrogen peroxide as the terminal oxidant. The highest activity and yield were achieved in the presence of iron(III) chloride. Cyclic β-ketoesters could be smoothly hydroxylated in 75–90% yield. For linear β-ketoester and β-ketoamide, the chloro-substituted products were obtained.
  • Keywords
    Iron catalysis , Ketoester , Selective oxidation , Hydrogen peroxide
  • Journal title
    Tetrahedron Letters
  • Serial Year
    2008
  • Journal title
    Tetrahedron Letters
  • Record number

    1861133