Title of article
2,2,3,3,11,11,12,12-Octamethyl-1,4,7,10,13-pentaoxacyclohexadecane: improved synthesis and crystal structure with NaSCN
Author/Authors
Loustau-Chartez، نويسنده , , Fanny and Robeson، نويسنده , , Rachel M. and Custelcean، نويسنده , , Radu and Sachleben، نويسنده , , Richard A. and Bonnesen، نويسنده , , Peter V.، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2009
Pages
3
From page
2936
To page
2938
Abstract
An efficient synthesis of 2,2,3,3,11,11,12,12-octamethyl-1,4,7,10,13-pentaoxacyclohexadecane (1, OM16C5) is described, which affords over an order of magnitude improvement in yield over the previously reported method. The first X-ray crystal structure of 1, as a complex with NaSCN, is also reported.
Keywords
Crown ether , 16-Crown-5 , sodium , improved synthesis
Journal title
Tetrahedron Letters
Serial Year
2009
Journal title
Tetrahedron Letters
Record number
1864074
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