Title of article
Synthesis and spin trapping properties of 1,1-dimethyl-3-(trifluoromethyl)-1H-isoindole N-oxide
Author/Authors
Hatano، نويسنده , , Bunpei and Miyoshi، نويسنده , , Katsunori and Sato، نويسنده , , Haruna and Ito، نويسنده , , Tomohiro and Ogata، نويسنده , , Tateaki and Kijima، نويسنده , , Tatsuro، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2010
Pages
3
From page
5399
To page
5401
Abstract
We have achieved an efficient synthesis of 1,1-dimethyl-3-(trifluoromethyl)-1H-isoindole N-oxide (2) in 39% yield by seven steps from 2-bromobenzoic acid (3). This compound serves as a spin trap reagent, giving a strong and stable ESR signal of the radical adduct of 2 in the presence of i-amyloxy radical generated by UV photolysis of i-amyl nitrite.
Journal title
Tetrahedron Letters
Serial Year
2010
Journal title
Tetrahedron Letters
Record number
1874969
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