Title of article :
A facile microwave assisted synthesis of spiro-1,3-oxazines from N-(2-(cyclohex-1-en-1-yl)ethyl)amides
Author/Authors :
Saikia، نويسنده , , Ujwal Pratim and Baruah، نويسنده , , Diganta and Pahari، نويسنده , , Pallab and Borah، نويسنده , , Manash Jyoti and Goswami، نويسنده , , Amrit and Konwar، نويسنده , , Dilip، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2014
Pages :
3
From page :
4328
To page :
4330
Abstract :
A mild and efficient methodology has been developed for the synthesis of spiro-1,3-oxazine derivatives by the microwave assisted cyclization of N-2-(1′-cyclohexenyl)ethyl-acetamides/benzamides. The reaction was catalyzed by in situ generated trimethylsilyl iodide and featured by its very short reaction time. The starting materials were easily obtained by the condensation of substituted acetic/benzoic acids with 2-(1′-cyclohexenyl)ethyl amine.
Keywords :
Spiroxazine , Microwave assisted synthesis , Trimethylsilyl iodide
Journal title :
Tetrahedron Letters
Serial Year :
2014
Journal title :
Tetrahedron Letters
Record number :
1890267
Link To Document :
بازگشت