Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance

We report here high-resolution 1H solid-state nuclear magnetic resonance spectra acquired by a combination of magic-angle spinning (MAS) and radiofrequency pulse methods up to MAS frequencies of 65 kHz. The details of the pulse methods and experimental conditions are outlined together with spectra from model compounds.