Title of article
Preparation, characterization and thermal decomposition mechanism of guanidinium azotetrazolate (GUZT)
Author/Authors
An، نويسنده , , Ting and Zhao، نويسنده , , Fengqi and Wang، نويسنده , , Qiong and Sheng، نويسنده , , Di-Lun and Pan، نويسنده , , Qing Yi Feng، نويسنده , , Hao and Yi، نويسنده , , Jian-Hua and Wang، نويسنده , , Ying-Lei، نويسنده ,
Pages
7
From page
405
To page
411
Abstract
Guanidinium azotetrazolate (GUZT) was prepared by replacement reaction using guanidine nitrate (GN) and 5-amino-tetrazole (5-AT) as raw materials. The morphology and structure of the title compound were characterized by scanning electron microscope (SEM), Fourier transform infrared (FTIR) spectroscopy and elementary analysis (EA). Thermal behaviors and thermal decomposition processes of GUZT were investigated by means of thermogravimetric thermogravimetric (TG) analysis, differential scanning colorimetry (DSC), condensed phase thermolysis/RSFT-IR and pyrogenetic mass spectrometry in a temperature-programmed mode. The thermal decomposition mechanisms of GUZT were obtained by analyzing its solid-phase thermal decomposition processes and gas-phase thermal decomposition products.
Keywords
thermal behavior , Physical chemistry , Guanidinium azotetrazolate , Thermal decomposition mechanism
Journal title
Astroparticle Physics
Record number
2036348
Link To Document