Title of article :
Analysis of electron intensity as a function of aperture size in energy-filtered transmission electron microscope imaging
Author/Authors :
Moore، نويسنده , , K.T and Howe، نويسنده , , J.M and Veblen، نويسنده , , D.R and Murray، نويسنده , , T.M and Stach، نويسنده , , E.A، نويسنده ,
Pages :
16
From page :
221
To page :
236
Abstract :
The dependence of electron intensity on condenser and objective aperture size in energy-filtered transmission electron microscope imaging was investigated using high-purity silicon. Results show that a reduction in intensity occurs in pre-edge and post-edge images due to a reduction in aperture size and that this effect depends more strongly on the objective aperture size (collection angle) than on the condenser aperture size. This reduction in intensity due to the use of a smaller objective aperture causes the signal in elemental maps of the Si L2,3 edge to decrease. However, although the signal decreases in both the pre-edge and post-edge images as either the condenser or objective aperture sizes decrease, the ratio of post-edge intensity to pre-edge intensity increases with decreasing objective aperture diameter, causing the value of the jump ratio to increase. This occurs because the effects of plural scattering on the background intensity decrease with objective aperture size and because the intensity reductions in the numerator (post-edge image intensity) and denominator (pre-edge image intensity) are similar, causing their ratio to increase as each decreases.
Keywords :
Electron energy-loss spectroscopy (EELS) , Aperture , Signal-to-background ratio (SBR) , Energy-filtered imaging (EFI) , Energy-filtering transmission electron microscopy (EFTEM) , Transmission electron microscopy (TEM) , Signal-to-noise ratio (SNR)
Journal title :
Astroparticle Physics
Record number :
2045249
Link To Document :
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