Title of article :
The preparation of (BEDO-TTF)2Cl·3H2O salt in Bu4NHgX3 + Bu4NX + 1,2-dichloroethane system. Shubnikov-de Haas oscillations
Author/Authors :
Zhilyaeva، نويسنده , , E.I. and Torunova، نويسنده , , S.A. and Lyubovskaya، نويسنده , , R.N. and Konovalikhin، نويسنده , , S.V. and Dyachenko، نويسنده , , O.A. and Lyubovskii، نويسنده , , R.B. and Pesotskii، نويسنده , , S.I.، نويسنده ,
Issue Information :
دوماهنامه با شماره پیاپی سال 1996
Abstract :
Electrochemical oxidation of BEDO-TTF (bis(ethylenedioxo)tetrathiafulvalene) in 1,2-dichloroethane in the presence of Bu4NHgX3 + Bu4NX (X = I, Br, Cl) as a supporting electrolyte at low current density results in the isolation of (BEDO-TTF)2Cl · 3H2O salt. Its composition has been established by a chemical analysis (Cl, C, H), electron probe microanalysis and X-ray analysis. The temperature dependence of the resistance has been studied down to 1.5 K at a pressure up to 30 kbar and at room temperature up to 80 kbar. Field and angular dependences of magnetoresistance have been investigated.
Keywords :
Electrocrystallization , crystal structure , Conductivity , Bis(ethylenedioxo)tetrathiafulvalene , Magnetotransport
Journal title :
Synthetic Metals
Journal title :
Synthetic Metals