Title of article
Synthesis of MoSe2 nanocrystallites by a solvothermal conversion from MoO3
Author/Authors
Zhan، نويسنده , , J.H. and Zhang، نويسنده , , Z.D. and Qian، نويسنده , , X.F. and Xie، نويسنده , , C.Wang Y and Qian، نويسنده , , Y.T، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 1999
Pages
5
From page
497
To page
501
Abstract
Nanocrystalline 2H–MoSe2 was prepared from MoO3, N2H4·H2O, and Se in pyridine at 300°C for 12 h by a solvothermal method. A gray-black product was collected and characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM) analysis. The XRD pattern showed that a phase-pure product was prepared. TEM analysis showed that the product was polycrystalline and had plate-shaped particles with a diameter of about 40 nm. The conversion process from MoO3 to MoSe2 is discussed.
Keywords
B. Chemical synthesis , A. Chalcogenides , A. Nanostructures , A. Layered compounds
Journal title
Materials Research Bulletin
Serial Year
1999
Journal title
Materials Research Bulletin
Record number
2094317
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