Title of article :
Polyol mediated synthesis of nanocrystalline M3SbS3 (M=Ag, Cu)
Author/Authors :
Chen، نويسنده , , Yin-di and Shen، نويسنده , , Guozhen and Tang، نويسنده , , Kaibin and Jiang، نويسنده , , Xuan and Huang، نويسنده , , Liying and Jin، نويسنده , , Yin and Qian، نويسنده , , Yitai، نويسنده ,
Issue Information :
روزنامه با شماره پیاپی سال 2003
Abstract :
A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197 °C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.
Keywords :
Nanostructures , chemical synthesis , Electron microscopy
Journal title :
Materials Research Bulletin
Journal title :
Materials Research Bulletin
