Title of article
Structure, thermal and magnetic characterization of hydrothermal synthesized Li2CuP2O7 crystals
Author/Authors
Gopalakrishna، نويسنده , , G.S. and Mahesh، نويسنده , , M.J. and Ashamanjari، نويسنده , , K.G. and Prasad، نويسنده , , J. Shashidhara Prasad، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2008
Pages
8
From page
1171
To page
1178
Abstract
New lithium copper(II) pyrophosphate, Li2CuP2O7 crystals were synthesized by the hydrothermal technique at moderate temperature and pressure conditions. The as-synthesized compound was characterized by DTA/TGA, infrared radiation, single crystal XRD and magnetic susceptibility measurement. The compound has crystallized in monoclinic system with C2/c space group and cell parameters a = 15.3360(14) Å, b = 4.8733(13) Å, β = 114.8(1)°, V = 585.2(2) Å, having tunnel type of cavities in the structure. Thermal behaviour and structural coordination of the prepared materials were investigated, respectively, using DTA/TGA and FTIR measurements. Magnetic results have revealed; it is a frequency and temperature dependent prospective paramagnetic materials.
Keywords
D. Crystal structure
Journal title
Materials Research Bulletin
Serial Year
2008
Journal title
Materials Research Bulletin
Record number
2098817
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