On the interaction between slip dislocations and twins in HCP Zr

We investigate the effect of stored prismatic dislocations on the onset and growth of { 1   0   1 ¯   2 } and { 1   1   2 ¯   2 } twins in pure Zr. A set of temperature jump tests, some combined with a strain path changes, are performed here to exploit the fact that slip-dominated plastic behavior occurs at room temperature and twin-dominated plastic behavior at lower temperatures. In some of the tests the material is pre-strained to various levels at room temperature to introduce prismatic slip dislocations, and then reloaded at liquid nitrogen. In other tests the material is pre-strained at liquid nitrogen, to different levels and in different directions, to generate either { 1   0   1 ¯   2 } tensile or { 1   1   2 ¯   2 } compressive twins, and then reloaded at room temperature. These tests are interpreted with a recently developed dislocation-density based single crystal model in order to elucidate slip-twin interactions operating at the nanometer scale. Our analysis suggests that (1) stored dislocations increase the resistance for further slip and for { 1   1   2 ¯   2 } twin propagation, but not for { 1   0   1 ¯   2 } twin propagation; (2) the onset of { 1   1   2 ¯   2 } twinning is insensitive to the amount of stored dislocations; (3) substantial slip occurs within the twin oriented domains, which can either increase or decrease the hardening rate by comparison to the one without twins.