Title of article :
A convenient and efficient protocol for the synthesis of acylals catalyzed by Brّnsted acidic ionic liquids under ultrasonic irradiation
Author/Authors :
Borikar، نويسنده , , Sanjay P. and Daniel، نويسنده , , Thomas، نويسنده ,
Issue Information :
فصلنامه با شماره پیاپی سال 2011
Abstract :
The synthesis of acylals (1,1-diacetates) via the reactions of aldehydes with acetic anhydride was carried out in 85–97% yields at room temperature under ultrasound irradiation catalyzed by the Brønsted acidic ionic liquid [bmpy]HSO4. This method provides several advantages, such as solvent-free conditions, operational simplicity, higher yields, and reduced environmental consequences. The ionic liquid was recovered and reused.
Keywords :
solvent-free , 1-Diacetates , 1 , Acylals , Ultrasonic irradiation , 1-Butyl-3-methylpyridinium hydrogen sulfate , Ionic liquid
Journal title :
Ultrasonics Sonochemistry
Journal title :
Ultrasonics Sonochemistry