Title of article
Synthesis and characterization of 6-(hydroxymethyl)-14,16-dimethyl-13,14,16,17-tetrahydro-6H-13,17-epiminodibenzo[e,-l][1,4]dioxacyclotridecin-15(7H)-one
Author/Authors
Banaei ، Alireza - Payame Noor University , Karimi ، Soheyla - Payame Noor University , Nurbageri ، Negar - Payame Noor University
Pages
5
From page
359
To page
363
Abstract
New 6-(hydroxymethyl)-14,16-dimethyl-13,14,16,17-tetrahydro-6H-13,17- epiminodibenzo[e,l][1,4]dioxacyclotridecin-15(7H)-one(2a) was synthesized in good yield by the Petrenko-Kritchenko reaction of 2,2 -((3-hydroxypropane-1,2-diyl)bis- (oxy))bisbenzaldehyde(1a) with diethyl ketone in the mixture of ethanol and acetic acid as solventin the presence of ammonium acetate. The compounds were characterized by elemental analyses, IR, 1H-NMR, 13C-NMR and mass spectrometry.
Keywords
Petrenko , Kritchenko condensation , macrocyclic compound , bisaldehyde
Journal title
Iranian Chemical Communication
Serial Year
2016
Journal title
Iranian Chemical Communication
Record number
2461026
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