Title of article :
Effect of Synthesis Condition on the Growth of SWCNTsvia Catalytic Chemical Vapour Deposition
Author/Authors :
MONSHI TOUSSI, SETAREH Universiti Putra Malaysia - Institute of Advanced Technology - Advanced Materials Nanotechnology Laboratory, Malaysia , FAKHRU’L-RAZI, A. Universiti Putra Malaysia - Department of Chemical and Environmental Engineering, Malaysia , LUQMAN CHUAH, A. Universiti Putra Malaysia - Department of Chemical and Environmental Engineering, Malaysia , SURAYA, A.R. Universiti Putra Malaysia - Department of Chemical and Environmental Engineering, Malaysia
Abstract :
Single-walled carbon nanotubes (SWCNTs) were synthesized by catalytic chemical vapor deposition (CCVD) of ethanol (C2H5OH) over Fe-Mo-MgO catalyst by using argon as a carrier gas. The reaction conditions are important factors that influence the yield and quality of carbon nanotubes. The effects of temperature and flow rate of carrier gas were investigated to increase the yield of carbon nanotubes. The synthesized carbon nanotubes were characterized by scanning electron microscopy, transmission electron microscopy, X-Ray diffraction and thermo-gravimetric analysis. The results showed that the growth of carbon nanotubes was effectively influenced by the reaction ambience and the synthesis condition. The temperature and flow rate of carrier gas played a key role in the yield and quality of synthesized CNTs. The estimated yield of synthesized carbon nanotubes was almost over 70%.
Keywords :
nanotubes (CNTs) , catalytic chemical vapor deposition (CCVD) , Fe , Mo , MgO catalyst , synthesis , yield