Title of article
An Optimization Study for Transesterification of Palm Oil using Response Surface Methodology (RSM)
Author/Authors
WONG, Y. C. Universiti Putra Malaysia - Faculty of Science, Centre of Excellence for Catalysis Science and Technology - Department of Chemistry, Malaysia , TAN, Y. P. Universiti Putra Malaysia - Faculty of Science, Centre of Excellence for Catalysis Science and Technology - Department of Chemistry, Malaysia , TAUFIQ-YAP, Y. H. Universiti Putra Malaysia - Faculty of Science, Centre of Excellence for Catalysis Science and Technology - Department of Chemistry, Malaysia , RAMLI, I. Universiti Putra Malaysia - Faculty of Science, Centre of Excellence for Catalysis Science and Technology - Department of Chemistry, Malaysia
From page
281
To page
290
Abstract
Biodiesel was produced via transesterification of palm oil with methanol in the presence of CaO-Nb2O5 mixed oxide catalyst. Response surface methodology (RSM) with central composite design (CCD) was performed to determine the optimum operating conditions and to optimize the biodiesel yield. In this study, the reaction variables being optimized were reaction time, catalyst loading and methanol to oil molar ratio. From the analysis of variance (ANOVA), the most influential parameter on biodiesel production was reaction time. The predicted yield was found in good agreement with the experimental value, with R²= 0.9902. The optimum biodiesel yield of 97.67% was achieved at 2.67 h reaction time, with 3.60 wt. % of catalyst and with methanol to oil molar ratio of 13.04. The high biodiesel yield can be correlated to the synergic effect of basicity between the metallic ions of CaO-Nb2O5 shown in the physicochemical analysis.
Keywords
Biodiesel , optimization , palm oil , RSM , transesterification
Record number
2556106
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