Title of article :
Synthesis And Characterization of 5-(Mercapto-1,3,4-Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid
Author/Authors :
Mahmoud, Muhanned J. University of Baghdad - College of Education For Pure Science(Ibn Al- Haitham) - Department of Chemistry, Iraq , AL-bayati, Redha I. Al-Mustansiriya University - College of Sciences - Department of Chemistry, Iraq , Saoud, Shaimaa A. University of Baghdad - College of Education For Pure Science(Ibn Al- Haitham) - Department of Chemistry, Iraq , Majeed, Ismaeel Y. University of Baghdad - College of Education For Pure Science(Ibn Al- Haitham) - Department of Chemistry, Iraq
Abstract :
5-(mercapto-1,3,4-thiadiazole-2yl)α,α-(diphenyl)methanol have been synthesized by ring closer of potassium xanthate[which have been prepared by reaction of benzilic acid hydrazide with carbon disulphide in potassium hydroxide] using conc.sulphuric acid at (0-5)°C scheme(I). Their characterization was carried out from T.L.C, M.P, FT.IR and ^1H-NMR.
Keywords :
1 , 3 , 4 , thiadiazole derivative
Journal title :
Ibn Alhaitham Journal For Pure and Applied Science
Journal title :
Ibn Alhaitham Journal For Pure and Applied Science
