Title of article :
Solid State 31P MAS NMR Detection of Hydrogen-bonded Phosphate Polymer in Calcium–Phosphate Composites
Author/Authors :
Ueyama، Norikazu نويسنده , , Takahashi، Kazuyuki نويسنده , , Doi، Mototsugu نويسنده , , Onoda، Akira نويسنده , , Okamura، Taka-aki نويسنده , , Yamamoto، Hitoshi نويسنده ,
Issue Information :
روزنامه با شماره پیاپی سال 2004
Abstract :
A novel poly(vinyl phosphate) ligand was synthesized as a model of biopolymer ligands containing the OH···O hydrogen bonds and CaHPO4·2H2O (brushite) composites with the polymer ligands were also prepared. Successful detection of the polymer ligand binding to the CaHPO4·2H2O crystals is achieved by 31P MAS NMR with 1 pda (single pulse with decoupling and phase cycling) sequence, which enhances 31P signals of the phosphate polymer having shorter T1 value.
Keywords :
Application-production research , Genetic-fuzzy system , grinding , Surface finish , Power requirement , prediction
Journal title :
CHEMISTRY LETTERS
Journal title :
CHEMISTRY LETTERS
