Analysis of deformation-induced crack tip toughening in ductile single crystals by nano-indentation

This paper reports on the experimental examination of the deformation characteristics near a crack tip in a cyclically work-hardened copper single crystal using a 2D surface scans with nano-indentation. The experimental methodology enables the characterization of the primary deformation field near a crack tip via the modulation of the imposed secondary deformation field by a nano-indentation. In a heavily deformed 4-point bend specimen, the measurements showed an existence of an asymptotic field around the crack tip at a distance of RP 2.5J/r0. The measurements also showed the qualitative details of toughness evolution within the high-gradient deformation field around the crack tip. The nature of dislocation distribution (i.e. statistically distributed vs. distributions necessitated by geometry) around the crack tip is quantified. The measurements indicate the dominance of the geometrically necessary dislocation within the finite deformation zone ahead of the tip up to a distance of R 3J/r0. Thereafter, it is confined in radial rays coinciding with the sector boundaries around the crack tip. These measurements elucidate the origin of the inhomogeneous hardening and the size dependent macroscopic response close to crack tip.