Trace element analysis by means of synchrotron radiation, XRF, and PIXE: selection of sample preparation procedure

Lattice parameter and thermal-expansion coefficient for magnesium nitride, Mg3N2, were determined using X-ray powder diffraction at the B2 beamline in Hasylab (DESY) in the temperature range from 11 K up to 304.5 K. The relative change of lattice parameter on raising the temperature in the studied range is about 0.14%. At 300 K, its value is 9.9644(1) ? and the linear thermal expansion coefficient derived from a polynomial approximation is a=1.1×10?5 K?1.