Author/Authors :
Esmaeili، Nazila نويسنده Faculty of Chemical and Petroleum Engineering, Sharif University of Technology, Tehran, I.R. IRAN , , Kazemiand، Hossein نويسنده Department of Chemical and Biochemical Engineering, Faculty of Engineering, The University of Western Ontario (UWO), London, Ontario, CANADA , , Bastani، Dariush نويسنده Faculty of Chemical and Petroleum Engineering, Sharif University of Technology, Tehran, I.R. IRANs ,
Abstract :
LTA Zeolite nanoparticles was successfully synthesized from clear solution under controlled conditions using hydrothermal method using tetramethyl ammonium hydroxide as a structural directing agent. The as-synthesized LTA zeolite particles were characterized by powder X-ray Diffraction (XRD) analysis, Scanning Electron Microscopy (SEM), Fourier Transform InfraRed (FT-IR) spectroscopy, Energy Dispersive X-ray (EDX) analysis and surface area measuring technique of Brunauer, Emmett and Teller (BET). XRD patterns and FT-IR spectra were ascertained the formation of pure crystalline phase of 4A (i.e. LTA) zeolite. SEM micrograph was shown particles size in the range of 60 -170 nm with uniform morphology.
The Si /Al ratio of the as-synthesized zeolite nanoparticles was 1.66 with a BET surface area of 421 m2/g.