Author/Authors :
Bagheri، Marziyeh نويسنده Department of Chemistry, Faculty of Science, Urmia University, Urmia 57159-165, Iran. , , Karimkoshteh، Mostafa نويسنده Department of Chemistry, Faculty of Science, Urmia University, Urmia 57159-165, Iran. ,
Abstract :
Nano silica-H2SO4 is an efficient and mild catalysis system for the regeneration of aldehyde from aldoximes. Ketoximes are converted to amides by Beckmann rearrangement in the presence of nano silica-H2SO4. The reactions are carried out in solvent-free conditions under microwave irradiation (600 W) within 50-120 sec in good yields.
