Author/Authors :
Yuji Mikata، نويسنده , , Kazumi Yoneda، نويسنده , , Tomoaki Tanase، نويسنده , , Isamu Kinoshita، نويسنده , , Matsumi Doe، نويسنده , , Fumiko Nishida، نويسنده , , Kenichi Mochida، نويسنده , , Shigenobu Yano، نويسنده ,
Abstract :
A useful preparation of an ethylenediamine derivative linked to d-glucose, 2,3-diaminopropyl β-d-glucopyranoside, has been described. The optically pure compound was obtained conveniently via recrystallization of the diastereomeric mixture of the diazido precursor. The stereochemistry of the ethylenediamino compound was elucidated by X-ray crystallography.
Keywords :
Diastereomer separation , Ethylenediamine , X-ray crystallography , Glucose
