• DocumentCode
    1059785
  • Title

    Interpretation of X-Ray Line Profile of Polycrystalline {\\hbox {MgB}}_{2}

  • Author

    Hanafusa, Kei ; Yamamoto, Akiyasu ; Ogino, Hiraku ; Horii, Shigeru ; Shimoyama, Jun-ichi ; Kishio, Kohji

  • Author_Institution
    Dept. of Appl. Chem., Univ. of Tokyo, Tokyo, Japan
  • Volume
    19
  • Issue
    3
  • fYear
    2009
  • fDate
    6/1/2009 12:00:00 AM
  • Firstpage
    2690
  • Lastpage
    2693
  • Abstract
    XRD peak profile analysis was performed on polycrystalline MgB2 bulks and tapes manufactured by various heat treatment conditions in order to investigate statistical value of crystallite size. Volume-weighted and area-weighted mean diameter of a bulk sample heated at 600degC for 6 h were estimated to be approximately 90 nm and 20 nm, respectively. These suggest that crystallite size distribution of MgB2 is very wide, although a lot of very small crystallites exist. Similar tendencies were observed for other samples. On the other hand J c values were found to be rather low compared to the expected values considering its small D a . This indicates that a small portion of crystallite interfaces act as effective pinning centers.
  • Keywords
    X-ray diffraction; critical current density (superconductivity); crystallites; flux pinning; grain size; heat treatment; magnesium compounds; sintering; superconducting critical field; superconducting materials; superconducting tapes; MgB2; X-ray line profile; area-weighted mean diameter; critical current density; crystallite size; flux pinning force; grain size; heat treatment; mono-core superconducting tapes; pinning centers; polycrystalline superconducting materials; powder-in-closed-tube method; sintering; temperature 600 C; time 6 h; upper critical field; volume-weighted mean diameter; Crystallite size; X-ray line profile analysis; magnesium diboride; polycrystalline bulks and tapes;
  • fLanguage
    English
  • Journal_Title
    Applied Superconductivity, IEEE Transactions on
  • Publisher
    ieee
  • ISSN
    1051-8223
  • Type

    jour

  • DOI
    10.1109/TASC.2009.2018116
  • Filename
    5067108